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- W130910264 abstract "The X-ray diffraction technique is applied to the detection and to the semiquantitative determination of some toxic dusts components commonly met in the iron and steelmaking industry. The calibration is carried out with standards obtained through wet or dry deposits of powders on cellulose nitrate filters. The diffractometer can work with samples rotating in an horizontal plane when the dust adherence on the filter is rather low, thanks to a special θ-θ device. The absorption correction is accounted for by comparing the diffracted intensities of the silver lines coming from a silver foil placed behind the filter, collected through the sample and through an unloaded filter. The method is applied to quartz and to ammonium sulphate. With quartz, concentrations of around 20 to 30 μg/cm2 may be determined with the available current equipment in the diffractometer technique. With ammonium sulphate the limit is higher, about 100 μg/cm2, due to factors inherent to the distribution of intensities in the diffraction patterns. Starting from these examples, a criterium is proposed for estimating the ability of a cristalline compound to be determined through microdiffraction." @default.
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- W130910264 date "1982-01-01" @default.
- W130910264 modified "2023-09-25" @default.
- W130910264 title "ANALYSIS OF MICROSAMPLES OF TOXIC DUSTS IN THE STEEL-MAKING INDUSTRY BY X-RAY DIFFRACTION" @default.
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- W130910264 doi "https://doi.org/10.1016/b978-0-08-028740-9.50038-0" @default.
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