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- W132237035 abstract "Abstract Conditions for separation and determination of diastereoisomers of cefuroxime axetil by HPTLC on cellulose layers with densitometry were developed. A good separation of the constituents was achieved using a mobile phase composed of 1 aqueous -cyclodextrinmethanol (15 + 1, v/v). For detecting spots on the chromatograms, densitometric measurements were used at 285 nm. The method is characterized by high sensitivity; the LOD was 0.04 g/spot and LOQ was 0.11 g/spot for both forms of the cefuroxime axetil diastereoisomers. For the individual diastereoisomers, high recovery values from 96.63 to 104.16 were obtained. Identification of the diastereoisomers was performed by 1H-NMR spectrometric analysis." @default.
- W132237035 created "2016-06-24" @default.
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- W132237035 date "2010-05-01" @default.
- W132237035 modified "2023-09-24" @default.
- W132237035 title "Chiral Separation of Diastereoisomers of Cefuroxime Axetil by High-Performance Thin-Layer Chromatography" @default.
- W132237035 doi "https://doi.org/10.1093/jaoac/93.3.771" @default.
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