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• W133745260 abstract "The enantioseparation of 2-aryloxypropionic acids by capillary electrochromatography was tested on columns with a monolithic stationary phase prepared from silanized fused-silica capillaries (100 microm I.D.) by in situ copolymerization of glycidyl methacrylate, ethylene glycol dimethacrylate and methyl methacrylate in the presence of formamide and 1-propanol as the porogen solvents. The porous chiral monolithic stationary phases were prepared by reaction of the epoxy-groups at the surface of the monolith with (+)-1-(4-aminobutyl)-(5R,8S,10R)-terguride. To attain the minimum HETP values for the enantiodiscrimination of 2-phenoxypropionic acid, the influence of the composition of polymerization solution on column total porosity and efficiency was investigated. Optimum mobile phase conditions were found for all analytes tested using acetonitrile-methanol mixtures containing triethylamine and acetic acid as the buffer components. Furthermore, the chemical and mechanical stabilities of the columns were satisfactory, allowing hundreds of analyses." @default.
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• W133745260 date "2006-07-01" @default.
• W133745260 modified "2023-10-03" @default.
• W133745260 title "Enantioseparation of 2-aryloxypropionic acids on chiral porous monolithic columns by capillary electrochromatography" @default.
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• W133745260 doi "https://doi.org/10.1016/j.chroma.2005.11.107" @default.
• W133745260 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/16364335" @default.
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