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- W140163921 abstract "Contaminated industrial effluents often contain a variety of organic pollutants which are difficult to analyze by standard GC/MS methods since often miss the more polar or nonvolatile of these organic compounds. The identification of highly polar analytes by chemical or rapid biological techniques is needed for characterization of the effluents. By correlating chemical characterization with toxicity a better picture of the effluent can be achieved. The present work will point out a master analytical protocol for determining a broad spectrum of organic analytes present in various industrial effluents from Europe (petrochemical plant and hazardous waste). The protocol consisted in the setup of a methodology based on solid-phase extraction for the preconcentration of a variety of pollutants: catechol, nitrophenols, pentachlorophenol, benzidines, acridine, phosphates, phthalates and nonionic detergents (nonyl phenol) followed by LC-MS characterization using Atmospheric Pressure Chemical Ionization (APCI) in the Positive and Negative Ion modes. The developed protocol permitted the unequivocal identification of target analytes like pentachlorophenol, tributyl phosphate, nonylphenol, dibutylphthalate, dimethylphthalate, bis(2-ethylhexyl)phthalate, tetramethyl thiourea, ethylbenzoate, 2-methylbenzenesulfonamide, isothiocyanate-cyclohexane, neopentyl glycol and 1methyl-2-pyrrolidinone present in industrial effluents. Three RaPID-magnetic particle-based ELISA kits for determining pentachlorophenol, carcinogenic PAHs and BTEX (benzene, toluene, ethylbenzene and o-, m- and p-xylene) were also applied to the characterization of the industrial effluents." @default.
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- W140163921 date "1998-01-01" @default.
- W140163921 modified "2023-10-15" @default.
- W140163921 title "A Master Analytical Protocol for Determining a Broad Spectrum of Organic Pollutants in Industrial Effluents" @default.
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- W140163921 doi "https://doi.org/10.1007/978-3-322-93454-3_7" @default.
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