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- W140932135 abstract "Two kinds of silanediol, 1-(triphenylmethyl)-1,1-dihydroxytrimthyldisiloxane (2a) and 1,2-bis(tri- phenylmethyl)-1,1,3,3-tetrahydroxydisiloxane (2b), were recrystallized from saturated acetone and diethyl ether solutions as single crystals suitable for X-ray crystallographic determination. In their single-crystal X-ray structures, the molecules of 2a and 2b crystallize in triclinic (a = 9.204 Å (α= 87.10(5)°), b = 12.496(7) Å (β= 81.50(4)°), c = 24.037(10) Å (γ= 74.25(3)°) in a unit cell) and triclinic (a = 9.2540(18) Å (α= 110.240(3)°), b = 14.169(3) Å (β= 106.902(3))°), c = 14.189(3) Å (γ= 101.092(4))° in a unit cell) space groups, respectively. X-ray single-crystal diffraction studies showed that the molecules of silanepolyols 2a and 2b in the solid state are regularly arranged through hydrogen-bonding and hydrophobic interactions. In their solid states, the remarkable hydrogen bondings of silanediol 2a with pyridine and 2b with water lead to one di- mensional columnar tube structures with hydrophilic cores, respectively. Such columnar tubes with hydro- philic cores are regularly packed through hydrophobic interactions of the organic/substituent of the silanediols." @default.
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- W140932135 date "2007-01-01" @default.
- W140932135 modified "2023-09-23" @default.
- W140932135 title "Note : Solid State Structures of Disiloxanediols. Hydrogen-Bonded Networked Structures" @default.
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