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- W145493967 abstract "Abstract In-tube extraction (ITEX) is a novel technique that can be coupled with gas-chromatography mass-spectrometry (GC-MS) and used for the extraction and separation of volatile compounds from different matrices. In this study a simple and efficient ITEX/GC-MS method was developed and optimized for the extraction and analysis of volatile compounds from tomatoes. The analytes were extracted from sample headspace by dynamic extraction and trapped into the selected sorbent material (Tenax TA), followed by their thermal desorption into the GC injector. Different extraction parameters were tested (incubation time and temperature, amount of sample, number of pumping strokes) and the optimal ones selected. The best compromised between the extraction performance and analysis time was achieved when 1g of sample was incubated at 70 o C for 20 min. followed by 30 extraction strokes. Between the main odor-active volatiles found in the analyzed cherry variety tomato samples were: hexanal, trans-2-hexenal, cis-3-hexenol, hexanol, 6-methyl-5-hepten-2-one, 2- and 3-methylbutanal, methyl salicylate, 1-penten-3-one. Keywords" @default.
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- W145493967 date "2012-01-01" @default.
- W145493967 modified "2023-10-18" @default.
- W145493967 title "ECO-FRIENDLY TECHNIQUE FOR TOMATOES VOLATILE FINGERPRINT DETERMINATION" @default.
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