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• W1482130758 endingPage "2932" @default.
• W1482130758 startingPage "2924" @default.
• W1482130758 abstract "The dialkyl complexes, [Zr{R(H)C(η5-C5Me4)(η5-C5H4)}R2′] (R = Pri, R′ = Me (2a), CH2Ph (3a); R = Bun, R′ = Me (2b), CH2Ph (3b); R = But, R′ = Me (2c), CH2Ph (3c); R = Ph, R′ = Me (2d), CH2Ph (3d)), have been synthesized by the reaction of the ansa-metallocene dichloride complex, [Zr{R(H)C(η5-C5Me4)(η5-C5H4)}Cl2] (R = Pri (1a), Bun (1b), But (1c), Ph (1d)), and two molar equivalents of the alkyl Gringard reagent. The insertion reaction of the isocyanide reagent, CNC6H3Me2-2,6, into the zirconium–carbon σ-bond of 2 gave the corresponding η2-iminoacyl derivatives, [Zr{R(H)C(η5-C5Me4)(η5-C5H4)}{η2-MeCNC6H3Me2-2,6}Me] (R = Pri (4a), Bun (4b), But (4c), Ph (4d)). The molecular structures of 1b, 1c and 3b have been determined by single-crystal X-ray diffraction studies." @default.
• W1482130758 created "2016-06-24" @default.
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• W1482130758 date "2006-06-01" @default.
• W1482130758 modified "2023-10-18" @default.
• W1482130758 title "Synthesis and reactivity of asymmetrically substituted ansa-bridged zirconocene complexes: X-ray crystal structures of [Zr{R(H)C(η5-C5Me4)(η5-C5H4)}Cl2] (R=Bun, But) and [Zr{Bun(H)C(η5-C5Me4)(η5-C5H4)}(CH2Ph)2]" @default.
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• W1482130758 doi "https://doi.org/10.1016/j.jorganchem.2006.02.039" @default.
• W1482130758 hasPublicationYear "2006" @default.
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