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- W1483815724 abstract "Abstract A mild, general, and convenient palladium‐catalyzed direct arylation of the 5‐position of azoles with aryl bromides, efficiently promoted by tetrabutylammonium acetate, is described. 1‐Methylpyrazole, oxazole, and thiazole reacted at 70 °C in N , N ‐dimethylacetamide by using Pd(OAc) 2 as the catalyst precursor. Electron‐poor and ‐rich functional groups, including the free hydroxy group, are well tolerated in the electrophilic partner. A variety of 5‐aryl‐1‐methylimidazoles were also very efficiently obtained simply by raising the reaction temperature to 110 °C. This ligand‐free protocol was successfully applied to the one‐pot synthesis of two bioactive natural compounds, balsoxin and texaline, starting from oxazole by sequential direct arylation of the 5‐ and 2‐positions." @default.
- W1483815724 created "2016-06-24" @default.
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- W1483815724 date "2013-07-16" @default.
- W1483815724 modified "2023-10-16" @default.
- W1483815724 title "Mild Palladium-Catalyzed Regioselective Direct Arylation of Azoles Promoted by Tetrabutylammonium Acetate" @default.
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- W1483815724 doi "https://doi.org/10.1002/ejoc.201300704" @default.
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