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- W1486417423 abstract "As part of a study directed at the total synthesis of (9S)-9-dihydroerythronolide A, the C7-C15 sulfoxide, (2S, 3R, 4S, 5R, 6R, 7R)-3, 5-isopropylidenedioxy-7-(4-methoxybenzyloxy)-6-methoxymethoxy-1-phenylsulfinyl-2, 4, 6-trimethylnonane, was coupled with the C1-C6 aldehyde, (2R, 3S, 4S, 5R)-6-tert-butyldiphenylsilyloxy-3, 5-dimethyl-2, 4-isopropylidenedioxyhexanal, to give the C1-C15 hydroxysulfoxide, which was converted to the seco-acid via a stereocontrolled methylation at the C6 position. Macrocyclization of the seco-acid by Yamaguchi's method gave the 14-membered lactone, which was converted to (9S)-9-dihydroerythronolide A." @default.
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- W1486417423 date "1989-01-01" @default.
- W1486417423 modified "2023-09-23" @default.
- W1486417423 title "A stereoselective total synthesis of (9S)-9-dihydroerythronolide A via coupling between the right-half (C1-C6) aldehyde and the left-half (C7-C15) sulfoxide." @default.
- W1486417423 cites W1990920308 @default.
- W1486417423 doi "https://doi.org/10.1248/cpb.37.1167" @default.
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