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- W148646432 abstract "Voltammetric studies of nitrobenzene reduction on Cu, glassy carbon (GC) and Pb electrodes were carried out with a viewto ascertaLi the choice of cathode material for p-aminophenol synthesis. Lead was found to give irreproducible responsesdue to some electrochemical mixed potential processes. However, on Cu and GC electrodes, the electroreduction was foundto stop at the four electron stage in the first peak potential region which indeed is the condition required for phenylhydroxylamineformation. This conclusion was drawn based on voltammetric peak current calculations as well as the comparativevoltammetric studies of nitrobenzene and p- nitrophenol which is known to follow a 6 electron path. Comparing the voltammetriccurves on Cu and GC for nitrobenzene in alcoholic Hz SO4 medium, it is noticed that the hydrogen evolution processstarts at much more positive potentials on Cu as compared to GC. Since further reduction of phenyl hydroxylamine to theaniline along with Hz evolution would also occur on Cu, it is concluded that carbon electrode would be a better choice forp-aminophenol synthesis" @default.
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- W148646432 date "1988-01-01" @default.
- W148646432 modified "2023-09-24" @default.
- W148646432 title "Cathode material in the electrosynthesis of p-aminophenol from nitrobenzene-voltammetric approach" @default.
- W148646432 hasPublicationYear "1988" @default.
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