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• W1486988054 abstract "This paper is the first in a series describing the in situ surface characterization of platinum electrodes using H and Cu deposited at underpotentials. The surface of a Pt(100) electrode pretreated by simple flame annealing and quenching in aqueous sulfuric acid is shown to contain a high concentration of defects such as vacancies and self-adsorbed Pt atoms. Adsorbed hydrogen is more strongly bound at these defects than on a uniform Pt(100) surface. Potential cycling in 1 M HCl produces a higher concentration of defects, while oxide formation and reduction in 0.5 M H2SO4 has the opposite effect. The nature of (100)-like sites at a polycrystalline platinum electrode is also discussed." @default.
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• W1486988054 date "1982-10-01" @default.
• W1486988054 modified "2023-10-18" @default.
• W1486988054 title "Surface characterization of Pt electrodes using underpotential deposition of H and Cu" @default.
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• W1486988054 doi "https://doi.org/10.1016/0022-0728(82)85123-1" @default.
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