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- W1488262015 abstract "Ordered Mesoporous Materials (OMS) functionalised with alkyl sulfonic acid groups have been proved to be efficient esterification catalysts. Among them, materials having MCM-41 type structure exhibit the best performance. In this paper we report the synthesis and characterisation of SO 3 H-phenyl-MCM-41 materials and their catalytic activity in the esterification of glycerol with lauric and oleic acids. We have studied several synthesis parameters: the amount of phenyl groups, the presence of additional methyl groups and the sulfonation procedure of the phenyl gorups. The materials obtained have been characterised by XRD, Elemental Analysis, Nitrogen adsorption, TGA and TEM. Finally, it has been studied the influence of the different synthesis parameters on the behaviour of the catalysts in the mentioned reaction of esterification." @default.
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- W1488262015 date "2002-01-01" @default.
- W1488262015 modified "2023-10-18" @default.
- W1488262015 title "Synthesis, characterisation and catalytic activity of SO3H-phenyl-MCM-41 materials" @default.
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- W1488262015 doi "https://doi.org/10.1016/s0167-2991(02)80290-7" @default.
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