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• W1488267284 abstract "Abstract A synthetic approach to the methyl esters of Prostaglandin B 1 and Phytoprostanes 16‐B 1 ‐PhytoP (PPB 1 ‐I) and 9‐L 1 ‐PhytoP (PPB 1 ‐II) based on the modified Julia olefination of a formylcyclopentenone and an appropriately protected hydroxy sulfone has been developed. The cyclopentenones were efficiently prepared by intermolecular Pauson–Khand reaction of a (silyloxymethyl)alkyne. The sulfone counterpart was prepared by regioselective ring‐opening of the appropriate chiral epoxides by 2‐mercaptobenzothiazole. The protecting group for the alcohol functionality on the sulfone proved to be crucial. Protection as a tert ‐butyl ether was the best solution, giving better results than a tert ‐butyldimethylsilyl ether." @default.
• W1488267284 created "2016-06-24" @default.
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• W1488267284 creator A5091712777 @default.
• W1488267284 date "2013-02-06" @default.
• W1488267284 modified "2023-10-18" @default.
• W1488267284 title "General Approach to Prostanes B₁by Intermolecular Pauson-Khand Reaction: Syntheses of Methyl Esters of Prostaglandin B₁and Phytoprostanes 16-B₁-PhytoP and 9-L₁-PhytoP" @default.
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• W1488267284 doi "https://doi.org/10.1002/ejoc.201201442" @default.
• W1488267284 hasPublicationYear "2013" @default.
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