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- W1488328056 abstract "Most researchers attribute grain boundary embrittlement in electro-deposited Nickel (ED-Ni) to the presence of small quantities of Sulfur as an impurity. It occurs in a highly mobile form that segregates to the grain boundaries. Evaluation of Sulfur segregation requires that a sample be fractured through the grain boundaries. However, this action may not always be possible. ED-Ni is inherently tough at ambient temperature, especially if a low level of Sulfur was intentionally maintained. A new method was developed to study Sulfur and other migrant species to the grain boundaries, which also migrate to free surfaces. A test specimen is heated by a quartz lamp within the sample preparation chamber, allowing the mobile species to migrate to polished free surfaces. There the mobile species are analyzed using X-ray photoelectron spectroscopy (XPS) also known as Electron Spectroscopy for Chemical Analysis (ESCA)." @default.
- W1488328056 created "2016-06-24" @default.
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- W1488328056 date "2000-01-01" @default.
- W1488328056 modified "2023-09-27" @default.
- W1488328056 title "Segregation Behavior of Sulfur and Other Impurities Onto the Free Surfaces of ED-Ni Deposits" @default.
- W1488328056 hasPublicationYear "2000" @default.
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