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• W1488337029 abstract "A simple, fast, and effective HPLC-DAD method for the quantification of nilotinib in blood serum with and without dasatinib as the internal standard was developed and presented in this work. A simple protein precipitation extraction method leads to satisfactory recoveries, accuracies, and coefficients of variation as 83.9–96.8%, 95.8–105.1%, and 2.1–6.1%, respectively. A Marcherey-Nagel Lichrospher 100-5 RP8 250 × 4 mm column held at 40°C, a mobile phase of 0.05 M H3PO4/KH2PO4-acetonitrile (7:3, v/v) at a flow rate of 1 mL/min, and a diode array detector operated at a wavelength of 265 nm were used for the analysis of 50 µL prepared sample injected into the HPLC. A single run was completed in 20 min. The presented method has a limit of quantification of 0.20 µM and is linear between 0.20 and 10 µM. The possibility of its use for the nilotinib analysis without an internal standard is also discussed." @default.
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• W1488337029 date "2012-01-01" @default.
• W1488337029 modified "2023-10-06" @default.
• W1488337029 title "HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY WITH ULTRAVIOLET DETECTION AND PROTEIN PRECIPITATION AS A WAY OF QUANTITATIVE DETERMINATION OF NILOTINIB WITH AND WITHOUT INTERNAL STANDARD" @default.
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• W1488337029 doi "https://doi.org/10.1080/10826076.2011.636469" @default.
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