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- W1489730631 abstract "Three distinct crystal modifications of 2,4-hexadiynylene bis(N-ethylcarbamate), (1c) are isolated under different conditions. The conditions necessary for the growth of crystals of the different modifications are described and their melting and phase transitions determined by differential thermal analysis. X-Ray diffraction studies yielded unit cell dimensions for some modifications of the monomer 1c as well as the polymer 2c, but full structural analyses were impossible to obtain. Molecular models of 1c with different conformations have been constructed and shown to be compatible with the observed cell dimensions and solid-state reactivities. The thermal and radiation polymerization kinetics of the two reactive modifications of 1c were studied. Despite the fact that the thermal polymerization of modification I of 1c is not a single-phase process, the kinetics are well described by the crystal-strain model, this fit being clearly fortuitous. A more detailed study of the kinetics reveals a second-order behaviour and a model for a two-phase polymerization process is proposed." @default.
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- W1489730631 date "1983-05-01" @default.
- W1489730631 modified "2023-10-14" @default.
- W1489730631 doi "https://doi.org/10.1002/macp.1983.021840520" @default.
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