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- W1490361946 abstract "A new synthetic route has been exploited for the large-scale production of 3'-deoxykanamycin A. The key stage in the synthesis involves the formation of the 3', 4'-anhydro-3'-epi derivative (9) or 2', 3'-anhydro-3'-epi derivative (10) followed by conversion to the 3'-deoxy derivative by reduction with Raney-nickel or sodium borohydride. Compound (9) or (10) was prepared by the treatment of 2', 2-di-O-benzoyl-3'-O-methylsulfonyl-tetra-N-ethoxycarbonylkanamycin A with sodium methoxide." @default.
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- W1490361946 date "1981-01-01" @default.
- W1490361946 modified "2023-09-27" @default.
- W1490361946 title "Deoxygenation of amino-glycoside antibiotics via anhydro intermediates. III. New synthesis of 3'-deoxykanamycin A." @default.
- W1490361946 doi "https://doi.org/10.1248/cpb.29.3469" @default.
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