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• W1490476772 abstract "[11C]MENET, a promising norepinephrine transporter imaging agent, was prepared by Suzuki cross coupling of 1 mg N-t-Boc pinacolborate precursor with [11C]CH3I in DMF using palladium complex generated in situ from Pd2(dba)3 and (o-CH3C6H4)3P together with K2CO3 as the co-catalyst, followed by deprotection with trifluoroacetic acid. This improved radiolabeling method provided [11C]MENET in high radiochemical yield at end of synthesis (EOS, 51 ± 3%, decay-corrected from end of 11CH3I synthesis, n = 6), moderate specific activity (1.5–1.9 Ci/µmol at EOS), and high radiochemical (>98%) and chemical purity (>98%) in a synthesis time of 60 ± 5 min from the end of bombardment. Copyright © 2013 John Wiley & Sons, Ltd." @default.
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• W1490476772 date "2013-04-24" @default.
• W1490476772 modified "2023-09-27" @default.
• W1490476772 title "An improved synthesis of [11C]MENET via Suzuki coupling with [11C]methyl iodide" @default.
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• W1490476772 doi "https://doi.org/10.1002/jlcr.3047" @default.
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