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- W1490784028 abstract "By chlorination of ethyltrichlorosilane and diethyldichlorosilane with Cl2 under UV irradiation, (pentachloroethyl)trichlorosilane and bis(pentachloroethyl)-dichlorosilane have been prepared, which react with powdered copper forming (trichlorovinyl)trichlorosilane and bis(trichlorovinyl)dichlorosilane. The derivatizations of these silanes at the silicon atom by use of phenylmagnesium bromide, trifluoro-methanesulfonic acid, lithium aluminium hydride, zinc difluoride and bromoform are described. (Trifluorovinyl)-, bis(trifluorovinyl)- and tris(trifluorovinyl)silanes have been prepared by the reaction of trifluoromethanesulfonyloxysilanes and trifluorovinyl-lithium. Attempts to prepare Si polymers bearing perhalovinyl groups by dehydrogenative coupling of RSiH2 with metal catalysts have not been successful." @default.
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- W1490784028 date "2000-01-17" @default.
- W1490784028 modified "2023-09-23" @default.
- W1490784028 title "Synthesis of Heavily Halogenated Vinylsilanes" @default.
- W1490784028 cites W1998080525 @default.
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- W1490784028 doi "https://doi.org/10.1002/9783527619917.ch36" @default.
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