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• W1497259178 abstract "Abstract Nanocubes of mixed‐crystal perovskites SrTi 1– x Zr x O 3 ( x = 0.25–0.6) were obtained in a two‐phase oil/water solvothermal environment. In an optically transparent autoclave, the evolution of an alkali metal oleate phase at the oil/water interface was monitored; this phase is the environment for nucleation and growth of the nanocrystals. The typical synthesis yields monodisperse nanocubes with an edge length of 10 nm. The size and shape of the nanoparticles do not depend on the Zr content and, most remarkably, do not vary with reaction time. We propose a growth mechanism that depends on the accessibility of the metal hydroxyalkanoate monomers to the growing crystal: after the formation of {100} facets, they are densely capped by oleate ion surfactants, and monomers are no longer able to attach. Increasing the reaction time only increases the amount of nanoparticles formed. As determined by Raman spectroscopy and energy‐dispersive X‐ray spectroscopy, the nanoparticles have the cubic ( Pm $bar {3}$ m ) perovskite structure and have an excess of B‐site ions (Ti + Zr), which is explained by a terminating Ti/Zr + O surface layer of the nanocubes. The monodisperse particles self‐assemble to form monolayers on a support." @default.
• W1497259178 created "2016-06-24" @default.
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• W1497259178 date "2014-12-12" @default.
• W1497259178 modified "2023-10-16" @default.
• W1497259178 title "Synthesis of Monodisperse SrTi _{1– <i>x</i>} Zr <i> _x </i> O ₃ Nanocubes in Oleate by a Two‐Phase Solvothermal Method" @default.
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• W1497259178 doi "https://doi.org/10.1002/ejic.201402724" @default.
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