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• W1499381738 abstract "Abstract Previously unknown 3,4‐diamino‐1,2,5‐selenadiazole ( 6 ) was prepared by hydrolysis of [1,2,5]selenadiazolo[3,4‐ c ][1,2,5]selenadiazole ( 7b ) and used in synthesis of novel 1,2,5‐selenadiazolo[3,4‐ b ]pyrazines by the Koerner–Hinsberg reaction covering the parent compound 4 and its substituted derivatives 5a – g . The compounds synthesized were characterized by solution and solid‐state 77 Se NMR, and 6 , 5‐Ph and 5,6‐Me 2 [1,2,5]selenadiazolo[3,4‐ b ]pyrazines ( 5a , g , respectively) by X‐ray diffraction. Electrochemical reduction of 5,6‐R 2 [1,2,5]selenadiazolo[3,4‐ b ]pyrazines 5c , g (R = Ph, Me) into novel persistent radical anions (RAs) was studied by cyclic voltammetry and the RAs [ 5c ] – and [ 5g ] – were characterized by EPR spectroscopy combined with DFT calculations." @default.
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• W1499381738 date "2015-07-23" @default.
• W1499381738 modified "2023-10-10" @default.
• W1499381738 title "[1,2,5]Selenadiazolo[3,4-<i>b</i>]pyrazines: Synthesis from 3,4-Diamino-1,2,5-selena­diazole and Generation of Persistent Radical Anions" @default.
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• W1499381738 doi "https://doi.org/10.1002/ejoc.201500742" @default.
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