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• W1502965513 abstract "[151515-23-0] C11H20N2 (MW 180.29)InChI = 1S/C11H21IN2/c1-8(2)12-14-7-13(9(3)4)10(5)11(14)6/h8-9,12H,1-6H3InChIKey = NOOSYWWJOSYXOF-UHFFFAOYSA-NPhysical Data: pale yellow solid, mp 190 °C (dec.).Solubility: soluble in toluene, benzene, THF, CH2Cl2, and scCO2.Form Supplied in: not commercially available.Analysis of Reagent Purity: not reported.Preparative Methods: the title compound (IPrMe 1) is most commonly prepared using procedures reported by Kuhn that involve the reduction of 1,3-diisopropyl-4,5-dimethylimidazole-2(3H)-thione using potassium in boiling THF.1 The thione itself is prepared by the condensation of diisopropyl thiourea and 3-hydroxy-2-butanone. In addition, deprotonation of the imidazolium salt using modifications to procedures originally reported by Arduengo have also been used.2, 3Handling, Storage, and Precautions: indefinitely stable under an inert atmosphere at ambient temperature." @default.
• W1502965513 created "2016-06-24" @default.
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• W1502965513 date "2014-05-27" @default.
• W1502965513 modified "2023-09-26" @default.
• W1502965513 title "1,3-Dihydro-4,5-dimethyl-1,3-bis(1-methylethyl)-2H-imidazol-2-ylidene" @default.
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• W1502965513 doi "https://doi.org/10.1002/047084289x.rn01656" @default.
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