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• W1503621824 abstract "The crystal structure of a (4S)-configured ammoniumproline derivative is presented. The trifluoroacetic acid salt of the acetylated methylester of (4S)-aminoproline (Ac-(4S)Amp-OMe) crystallized as the trans conformer with a C(4)-endo ring pucker. The high-resolution structure shows typical parameters for a transannular H-bond and an n → π* interaction between the adjacent amide and ester groups. The structure corroborates previous findings of solution phase studies on the importance of these two interactions in acidic and neutral aqueous environments for the conformation of this pH-responsive proline derivative. Copyright © 2015 European Peptide Society and John Wiley & Sons, Ltd." @default.
• W1503621824 created "2016-06-24" @default.
• W1503621824 creator A5030172234 @default.
• W1503621824 creator A5042327776 @default.
• W1503621824 creator A5073517394 @default.
• W1503621824 date "2015-01-08" @default.
• W1503621824 modified "2023-09-23" @default.
• W1503621824 title "Crystal structure of (4<i>S</i> )-aminoproline: conformational insight into a pH-responsive proline derivative" @default.
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• W1503621824 doi "https://doi.org/10.1002/psc.2734" @default.
• W1503621824 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/25581874" @default.
• W1503621824 hasPublicationYear "2015" @default.
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