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- W1506435679 abstract "In order to elucidate the stereochemistry of 14-membered macrolactone, an X-ray crystal structural analysis of p-bromobenzoylpikromycin (C35H50O9NBr·H2O) was carried out. The crystals are monoclinic with space group P21 and unit cell dimensions of a=19.027 (9) A, b=14.876 (5) A, c=7.148 (3) A, β=108.97 (8)°, Z=2. The crystal structure was solved by the heavy-atom method and refined by the block-diagonal least-squares method including anisotropic thermal parameters to a final R value of 0.118. The absolute configuration of pikromycin was determined on the D-desosamine moiety to be 2R, 4R, 5S, 6S, 8R, 12S, 13R, and 10E. A new diamond latticeconformation model D for p-bromobenzoylpikromycin is proposed based on the result of X-ray analysis." @default.
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- W1506435679 date "1977-01-01" @default.
- W1506435679 modified "2023-10-17" @default.
- W1506435679 title "Stereochemistry of macrolides. II. Crystal structure of p-bromobenzoylpikromycin." @default.
- W1506435679 doi "https://doi.org/10.1248/cpb.25.2385" @default.
- W1506435679 hasPublicationYear "1977" @default.
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