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• W1507704369 abstract "The layered rock salt material with the structure loses up to of its oxygen reversibly at high temperature. It transforms initially to a second layered structure, , that may be associated with cooperative Jahn-Teller distortion of ions and considerable interlayer cation mixing. By continuous disordering and further oxygen loss, it finally transforms into a simple cubic rock salt structure above 1000°C, as shown by thermogravimetry and high-temperature X-ray powder diffraction. X-ray absorption near-edge structure results confirm that oxygen deficiency induces reduction of mainly Mn and to a small extent Ni, commencing with the fully oxidized stoichiometry . This correlates with oxygen contents determined by thermogravimetry and Rietveld refinement of powder X-ray diffraction data, with oxidation states determined by chemical titration and with electrochemical behavior during cycling. The cycling results show that samples with the structure have better performance and capacity than those with and especially structures and that the , capacity decreases with increasing oxygen deficiency δ." @default.
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• W1507704369 date "2007-01-01" @default.
• W1507704369 modified "2023-10-16" @default.
• W1507704369 title "Oxygen Stoichiometry-Structure-Property Correlations in Li[sub 2∕3][Mn[sub 2∕3]Ni[sub 1∕3]]O[sub 2−δ] with O[sub 3] Structure" @default.
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• W1507704369 doi "https://doi.org/10.1149/1.2742901" @default.
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