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- W1509430812 abstract "The mixed compound potassium–ammonium mercurate exhibits two phase transitions at T1=395 K and T2=424 K:phaseI−(395K)→phaseII−(424K)→phaseIIIThese transitions have been detected by differential scanning calorimetry, X-ray diffraction and Raman scattering on polycrystalline samples of K2.51(NH4)1.49Hg3Cl10.2H2O. The room temperature phase has space group Pmcm (a=4.511(4) Å, b=14.489(9) Å and c=16.074(12) Å). Phase II is disordered and exhibits orthorhombic symmetry (a=4.500(1) Å, b=17.758(5) Å and c=22.895(5) Å). Hydrogen bonding, the nature and the degree of structure (dis)order and the mechanisms of the phase transitions are discussed. The NH4+ ions show an important orientation disorder at the high temperatures." @default.
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- W1509430812 date "1999-03-01" @default.
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- W1509430812 title "DSC, X-Ray diffraction and Raman studies in the compound K2.51(NH4)1.49Hg3Cl10.2H2O" @default.
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- W1509430812 doi "https://doi.org/10.1016/s0925-8388(98)00912-8" @default.
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