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- W1509940658 abstract "The cationic polymerization of isobutyl vinyl ether (IBVE) was examined using various Lewis acids in the presence of an excess of acetylacetone (acac). With EtAlCl2, TiCl4, and FeCl3, almost no polymerization proceeded when the acac concentration was over 0.5 M. In contrast, SnCl4, ZnCl2, and GaCl3 induced polymerization even at a higher acac concentration. Interestingly, SnCl4 produced polymers with a narrow molecular weight distribution (MWD). In addition, the number-average molecular weight (Mn) of the product polymers increased proportionally to the monomer conversion. It should also be noted that the Mn of the products varied inversely with the amounts of SnCl4. These results suggested that H+, which was generated by the coordination of an acac molecule with SnCl4, is the real initiator for the polymerization." @default.
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- W1509940658 date "2011-01-01" @default.
- W1509940658 modified "2023-09-23" @default.
- W1509940658 title "Living Cationic Polymerization of Vinyl Ether with a Lewis Acid/Acetylacetone Initiating System—The Role of Acetylacetone as a Protogen and a Ligand" @default.
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- W1509940658 doi "https://doi.org/10.1295/koron.68.349" @default.
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