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• W1512954345 abstract "57Fe and 119Sn Mössbauer data are reported for mono- and bis-triorganostannyl ferrocenes together with 119Sn NMR chemical shifts. The reactions of bis-triphenyl-stannylferrocene Fc(SnPh3)2 with various electrophiles have been studied. Acid cleavage occurred with both FcSn and PhSn bond fission. In contrast, mercuri-destannylation with HgCl2 gave only Fc(HgCl)2. Iodination gave a mixture of the mono- and bis-iodides Fc(SnPh3)(SnPh2I)2 and Fc(SnPh2I)2 resulting from dominant PhSn cleavage. Oxidation of Fc(SnPh3)2 by FeCl3 required more than one equivalent of oxidant. The 57Fe and 119Sn Mössbauer spectra of the resultant ferrocinium ion was notable for the appearance of a measurable quadrupole splitting in both cases; this is discussed in terms of polar and steric effects." @default.
• W1512954345 created "2016-06-24" @default.
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• W1512954345 date "1986-04-01" @default.
• W1512954345 modified "2023-10-17" @default.
• W1512954345 title "Mössbauer studies on ferrocene complexes" @default.
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• W1512954345 doi "https://doi.org/10.1016/0022-328x(86)82041-1" @default.
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