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• W1517324740 abstract "This chapter discusses thermal analysis. Thermal analysis measurements are conducted for the purpose of evaluating the physical and chemical changes that may take place in a sample as a result of thermally induced reactions. This requires interpretation of the events observed in a thermogram in terms of plausible thermal reaction processes. The reactions normally monitored can be endothermic (melting, boiling, sublimation, vaporization, desolvation, solid–solid phase transitions, or chemical degradationor exothermic (crystallization or oxidative decomposition) in nature. Thermal methods have found extensive use in the past as part of a program of preformulation studies because carefully planned work can be used to indicate the existence of possible drug–excipient interactions in a prototype formulation. Thermal methods of analysis can be used to evaluate compound purity, polymorphism, solvation, degradation, drug–excipient compatibility, and a wide variety of other thermally related characteristics. Differential thermal analysis (DTA) consists of the monitoring of the difference in temperature existing between a solid sample and a reference as a function of temperature. The chapter describes the methodology appropriate for the measuring of DTA profiles. A schematic diagram illustrating the essential aspects of the DTA technique is also shown in the chapter." @default.
• W1517324740 created "2016-06-24" @default.
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• W1517324740 date "2006-01-01" @default.
• W1517324740 modified "2023-10-16" @default.
• W1517324740 title "Chapter 4 Thermal analysis" @default.
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• W1517324740 doi "https://doi.org/10.1016/s0166-526x(06)47004-5" @default.
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