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- W1519184552 abstract "The melting behaviour of drawn and undrawn nylon 6 annealed from 80 to 228°C for 6 h in vacuum is studied by means of DSC and X-ray scattering. The melting behaviour is interpreted in terms of growth and perfection of crystallites during annealing. The equilibrium melting point Tm0 = (254 ± 3)°C as well as the specific surface free energy σe = 33 erg/cm2 are calculated from the crystallite size data by applying the Thomson equation for drawn and undrawn samples. The heat of fusion of an infinitely large crystal ΔH0 = (188 ± 8) J/g is estimated too. Das Schmelzverhalten von gerecktem und ungerecktem Polyamid 6, das 6 h im Vakuum im Bereich von 80 bis 228°C getempert worden war, wurde mittels Differential-Scanning-Kalorimetrie und Röntgenbeugung untersucht. Das Schmelzverhalten wird an Hand der Größe und Perfektion der Kristallite beim Tempern interpretiert. Der Gleichgewichtsschmelzpunkt Tm0 = (254 ± 3)°C sowie die spezifische freie Oberflächenenergie σe = 33 erg/cm2 wurden aus den Kristallitgrößen von gereckten und ungereckten Proben mit Hilfe der Thomson-Gleichung berechnet. Weiterhin wurde die Schmelzwärme des unendlich großen Kristalls zu ΔH0 = (188 ± 8)J/g abgeschätzt." @default.
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- W1519184552 date "1981-06-01" @default.
- W1519184552 modified "2023-10-14" @default.
- W1519184552 doi "https://doi.org/10.1002/actp.1981.010320606" @default.
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