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- W1520357941 abstract "Morphological studies on graphite surfaces by scanning electron microscopy are presented for platforms made from total pyrolytic graphite, and for polycrystalline electrographite tubes with pyrographite coating in which the pyrolytic graphite platforms are inserted. Platforms made of pyrolytic graphite have a very long lifetime and can actually survive several tubes. But also the lifetime of polycrystalline electrographite tubes with pyrographite coating is substantially longer when the sample is deposited on a platform and not on the tube wall. The analytically useful lifetime of platform and tube comes close to 1000 determinations at an atomization temperature of 2650°C, and even in the presence of corrosive matrices 500 determinations can be performed without significant loss in sensitivity. Intercalation appears to be no problem with pyrolytic graphite platforms. Substantial deposition of graphite was found on the platform under different analytical conditions, leading to a secondary coating of the surface. The sensitivity of carbide-forming elements depends very much upon the quality of the pyrographite coating of the polycrystalline electrographite tubes in which the platforms are mounted." @default.
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- W1520357941 date "1986-01-01" @default.
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- W1520357941 title "Scanning electron microscopy studies on surfaces from electrothermal atomic absorption spectrometry" @default.
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- W1520357941 doi "https://doi.org/10.1016/0584-8547(86)80069-6" @default.
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