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• W1520694895 abstract "NMR signals of surface nuclei of solids may be enhanced by the transfer of spin polarization from laser-polarized noble gases. Until now such experiments have not been feasible under conditions of magic angle spinning. In the present contribution it is shown that laser-polarized129Xe can be inserted into a spinning rotor under continuous-flow conditions using helium as a carrier gas. Effective adsorption of xenon on the sample occurs at temperatures of about 163–173 K making possible the observation of a spin polarization induced nuclear Overhauser effect (SPINOE) from the laser-polarized129Xe to surface1H nuclei of SiO2(AEROSIL300). This technique opens the way to selectively enhancedhigh-resolutionmultinuclear surface NMR experiments." @default.
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• W1520694895 date "1998-01-01" @default.
• W1520694895 modified "2023-09-25" @default.
• W1520694895 title "Surface NMR Using Laser-Polarized129Xe under Magic Angle Spinning Conditions" @default.
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• W1520694895 doi "https://doi.org/10.1006/jmre.1997.1296" @default.
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