Matches in SemOpenAlex for { <https://semopenalex.org/work/W1520960064> ?p ?o ?g. }
Showing items 1 to 96 of
96
with 100 items per page.
- W1520960064 endingPage "320" @default.
- W1520960064 startingPage "316" @default.
- W1520960064 abstract "A total reflection X-ray fluorescence (TXRF) method for the determination of chlorine at trace levels in nuclear fuel samples is described. Chlorine present in trace concentrations in nuclear fuel materials such as U3O8, (U,Pu)C, PuO2 and Pu-alloys was first separated from the solid matrix by pyrohydrolysis as HCl and was collected in 5 mM NaOH solution. This solution was analyzed for chlorine by TXRF spectrometry using Cl Kα analytical line excited by W Lα. Cobalt was used as internal standard. The precision for such chlorine determination was found to be within 27% (n = 4) when the analysis was carried out in air atmosphere. This could be improved to 8% by making TXRF measurement in flowing helium atmosphere. The results obtained from TXRF determinations were also compared with those obtained from ion chromatography (IC) and were in good agreement. The collection of distillate during pyrohydrolysis in NaOH helped in counterchecking loss of chlorine during TXRF sample preparation. The average deviation of TXRF-determined values in helium-purged TXRF measurements with IC determined values (as chloride) was 15% at a chlorine concentration level in the range of 1–70 µg/mL. Copyright © 2012 John Wiley & Sons, Ltd." @default.
- W1520960064 created "2016-06-24" @default.
- W1520960064 creator A5001638145 @default.
- W1520960064 creator A5026086747 @default.
- W1520960064 creator A5033103793 @default.
- W1520960064 creator A5035546284 @default.
- W1520960064 creator A5038787089 @default.
- W1520960064 creator A5057901318 @default.
- W1520960064 creator A5081506267 @default.
- W1520960064 date "2012-05-14" @default.
- W1520960064 modified "2023-09-26" @default.
- W1520960064 title "A total reflection X-ray fluorescence method for the determination of chlorine at trace levels in nuclear materials without sample dissolution" @default.
- W1520960064 cites W1486496099 @default.
- W1520960064 cites W1966796451 @default.
- W1520960064 cites W1989397163 @default.
- W1520960064 cites W1991451719 @default.
- W1520960064 cites W2009506365 @default.
- W1520960064 cites W2017323663 @default.
- W1520960064 cites W2039959034 @default.
- W1520960064 cites W2048704742 @default.
- W1520960064 cites W2072683824 @default.
- W1520960064 cites W2123548123 @default.
- W1520960064 cites W2323029718 @default.
- W1520960064 doi "https://doi.org/10.1002/xrs.2400" @default.
- W1520960064 hasPublicationYear "2012" @default.
- W1520960064 type Work @default.
- W1520960064 sameAs 1520960064 @default.
- W1520960064 citedByCount "25" @default.
- W1520960064 countsByYear W15209600642012 @default.
- W1520960064 countsByYear W15209600642013 @default.
- W1520960064 countsByYear W15209600642014 @default.
- W1520960064 countsByYear W15209600642015 @default.
- W1520960064 countsByYear W15209600642016 @default.
- W1520960064 countsByYear W15209600642017 @default.
- W1520960064 countsByYear W15209600642018 @default.
- W1520960064 countsByYear W15209600642019 @default.
- W1520960064 countsByYear W15209600642020 @default.
- W1520960064 crossrefType "journal-article" @default.
- W1520960064 hasAuthorship W1520960064A5001638145 @default.
- W1520960064 hasAuthorship W1520960064A5026086747 @default.
- W1520960064 hasAuthorship W1520960064A5033103793 @default.
- W1520960064 hasAuthorship W1520960064A5035546284 @default.
- W1520960064 hasAuthorship W1520960064A5038787089 @default.
- W1520960064 hasAuthorship W1520960064A5057901318 @default.
- W1520960064 hasAuthorship W1520960064A5081506267 @default.
- W1520960064 hasConcept C113196181 @default.
- W1520960064 hasConcept C121332964 @default.
- W1520960064 hasConcept C147789679 @default.
- W1520960064 hasConcept C162170617 @default.
- W1520960064 hasConcept C162356407 @default.
- W1520960064 hasConcept C177322064 @default.
- W1520960064 hasConcept C178790620 @default.
- W1520960064 hasConcept C185592680 @default.
- W1520960064 hasConcept C2778695967 @default.
- W1520960064 hasConcept C43617362 @default.
- W1520960064 hasConcept C505241676 @default.
- W1520960064 hasConcept C546029482 @default.
- W1520960064 hasConcept C62520636 @default.
- W1520960064 hasConcept C88380143 @default.
- W1520960064 hasConcept C91881484 @default.
- W1520960064 hasConceptScore W1520960064C113196181 @default.
- W1520960064 hasConceptScore W1520960064C121332964 @default.
- W1520960064 hasConceptScore W1520960064C147789679 @default.
- W1520960064 hasConceptScore W1520960064C162170617 @default.
- W1520960064 hasConceptScore W1520960064C162356407 @default.
- W1520960064 hasConceptScore W1520960064C177322064 @default.
- W1520960064 hasConceptScore W1520960064C178790620 @default.
- W1520960064 hasConceptScore W1520960064C185592680 @default.
- W1520960064 hasConceptScore W1520960064C2778695967 @default.
- W1520960064 hasConceptScore W1520960064C43617362 @default.
- W1520960064 hasConceptScore W1520960064C505241676 @default.
- W1520960064 hasConceptScore W1520960064C546029482 @default.
- W1520960064 hasConceptScore W1520960064C62520636 @default.
- W1520960064 hasConceptScore W1520960064C88380143 @default.
- W1520960064 hasConceptScore W1520960064C91881484 @default.
- W1520960064 hasIssue "5" @default.
- W1520960064 hasLocation W15209600641 @default.
- W1520960064 hasOpenAccess W1520960064 @default.
- W1520960064 hasPrimaryLocation W15209600641 @default.
- W1520960064 hasRelatedWork W1624124780 @default.
- W1520960064 hasRelatedWork W1975904626 @default.
- W1520960064 hasRelatedWork W1996936725 @default.
- W1520960064 hasRelatedWork W2023798840 @default.
- W1520960064 hasRelatedWork W2055079834 @default.
- W1520960064 hasRelatedWork W2120047210 @default.
- W1520960064 hasRelatedWork W2221902476 @default.
- W1520960064 hasRelatedWork W2319387468 @default.
- W1520960064 hasRelatedWork W2409754106 @default.
- W1520960064 hasRelatedWork W2520587148 @default.
- W1520960064 hasVolume "41" @default.
- W1520960064 isParatext "false" @default.
- W1520960064 isRetracted "false" @default.
- W1520960064 magId "1520960064" @default.
- W1520960064 workType "article" @default.