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- W1521543670 abstract "The preparation and spectral properties of twenty-five arylazocyanoacetarylamides (VI–VIII) are investigated. Analysis of the IR and UV spectra of such compounds (VI–VIII) shows that they are of the hydrazo rather than the azo form. The reaction of benzenediazonium ion and the arylazo derivatives (VI and VII) in the presence of sodium hydroxide (and not in the presence of sodium acetate) produces 3-cyano-1,5-diarylformazans (IX). A mechanism is suggested for the formation of formazans (IX). Reaction of (VI–VII) with Grignard reagents results in 1,2-addition to the cyanide group with the formation of arylazoiminoacylacetanilides (X), which were hydrolysed to the corresponding arylazoacylacetanilides (XI). The UV spectral properties of compounds X and XI are compared." @default.
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- W1521543670 date "1971-01-01" @default.
- W1521543670 modified "2023-10-11" @default.
- W1521543670 title "Cyanoacetarylamides—I" @default.
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- W1521543670 doi "https://doi.org/10.1016/s0040-4020(01)91641-2" @default.
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