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- W1521832448 abstract "The crystal structure of poly(chloromethyl ethylene oxide) or polyepichlorohydrin has been carried out, by X-ray diffraction technique. The parameters of the orthorhombic unit-cell are: a = 12.16 A, b = 4.90 A, c = 7.03 A, fairly coincident with those given by RICHARDS (Diss. Abstr. 22 (1961) 1029). Two space-groups are proposed: Pna21 and Pnam, the former being more probable. Chain conformation is exactly like that previously given by the authors for the poly-propylene-oxide. The side chloromethyl-group lies on a plane perpendicular to the chain axis, in accordance with the staggered bonds principle.Mit Hilfe der Rontgenbeugung wurde die Kristallstruktur von Poly-Epichlorhydrin ermittelt. Die Gitterkonstanten der orthorhombischen Elementarzelle sind: a = 12,16 A, b = 4,90 A und c = 7,03 A. Die Werte sind in ubereinstimmung mit den von RICHARDS (Diss. Abstr. 22 (1961) 1029) angegebenen. Es werden zwei Raumgruppen, namlich Pna21 und Pnam vorgeschlagen, wobei eine grosere Wahrscheinlichkeit fur die erstere spricht Die Kettenkonformation entspricht genau der von den Autoren schon fruher fur das Poly-Epichlorhydrin angegebenen. Die Chlormethyl-Seitengruppen liegen in einer zur Kettenachse senkrechten Ebene, wie es dem Prinzip der „staggered bonds” entspricht" @default.
- W1521832448 created "2016-06-24" @default.
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- W1521832448 date "1970-04-07" @default.
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- W1521832448 doi "https://doi.org/10.1002/macp.1970.021330111" @default.
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