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- W1522333856 abstract "The four title compounds have been synthesized and characterized by 1H, 13C and 31P NMR spectroscopy and their identities confirmed by elemental analysis and X-ray crystallography. But2P(E)NHPrn [E=Se (1); E=Te (2)] and Ph2P(E)NHPrn [E=Se (3)] were prepared by the metathesis reaction of LiNHPrn with the appropriate chlorophosphine in diethylether at −78 °C, followed by reaction with elemental selenium or tellurium at reflux temperatures. (1) and (2) are isostructural with PSe 2.1163(14) Å and PTe 2.3642(13) Å. In (3) a PSe bond length of 2.1159(10) Å is observed. (4) was prepared by the additional of two equivalents of diethylchlorophosphine to the dilithium salt of n-propylamine." @default.
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- W1522333856 date "2004-07-01" @default.
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- W1522333856 title "Synthesis and characterization of chalcogenoic aminophosphines: X-ray structures of But2P(E)NHPrn (E=Se, Te), Ph2P(Se)NHPrn and {Et2P(Se)}2NPrn" @default.
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- W1522333856 doi "https://doi.org/10.1016/j.poly.2004.04.028" @default.
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