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- W1523017812 abstract "This chapter reviews that despite the success of proton nuclear magnetic resonance (H n.m.r.) spectroscopy as a tool for studying the structures of organic compounds in solution, the technique nevertheless suffers from a number of limitations. These limitations become increasingly serious with increase in the size and molecular complexity of the system of interest. The chapter discusses that when attention has been directed to studies of polymeric materials, especially those of biochemical relevance, much of the incisive power of the H n.m.r. technique has, to date, been lost. The outcome of this situation is clearly exemplified in the carbohydrate area, where H n.m.r. spectroscopy is generally the tool preferred for structural studies of mono-saccharide derivatives, and yet studies of polysaccharide derivatives have yielded relatively little structural information. The principal source of many of the limitations of H n.m.r, spectroscopy is the inherently low sensitivity of H chemical-shifts with respect to changes in chemical and stereochemical environment; as a result, the H n.m.r. spectra of polysaccharides and other polymers are often characterized by broadband consisting of overlapping resonances." @default.
- W1523017812 created "2016-06-24" @default.
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- W1523017812 date "1974-01-01" @default.
- W1523017812 modified "2023-10-14" @default.
- W1523017812 title "Solutions to The Hidden-Resonance Problem in Proton Nuclear Magnetic Resonance Spectroscopy" @default.
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- W1523017812 doi "https://doi.org/10.1016/s0065-2318(08)60247-4" @default.
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