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- W1524204557 abstract "In the presence of NBu4nBr acting as phase-transfer reagent, organosilicon trichloride RSiCl3 reacts in acetonitrile with the trivacant tungstophosphate sodium salt β-A-Na8H[PW9O34]·24 H2O to give hybrid organosilyl polyoxotungstate derivatives α-A-[NBu4n]3[PW9O34(RSiO)3(RSi)] (R=C2H3 (1), CH3 (2)). These compounds are characterized by X-ray crystallography. Each of the two hybrid anions consists of one α-A-PW9O349− framework on which is grafted by three RSiO groups through six SiOW bridges, each of which is attached to the fourth RSi through three SiOSi bridges. Both hybrid anions become saturated, close cage structure and display C3v symmetry." @default.
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- W1524204557 date "2003-05-01" @default.
- W1524204557 modified "2023-09-23" @default.
- W1524204557 title "Organosilyl derivatives of trivacant tungstophosphate of general formula α-A-[PW9O34(RSiO)3(RSi)]3−" @default.
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- W1524204557 doi "https://doi.org/10.1016/s0022-328x(03)00252-3" @default.
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