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• W1526119469 abstract "SummaryThe relationship between the mineralization of peritubular dentin (PTD) and intertubular dentin (ITD) is not well understood. Tubules are quite small, diameter ∼2 µm, and this makes the near-tubule region of dentin difficult to study. Here, advanced characterization techniques are applied in a novel way to examine what organic or nanostructural signatures may indicate the end of ITD or the beginning of PTD mineralization. X-ray fluorescence intensity (Ca, P, and Zn) and X-ray diffraction patterns from carbonated apatite (cAp) were mapped around dentintubules at resolutions ten times smaller than the feature size (200 nm pixels), representing a 36% increase in resolution over earlier work. In the near tubule volumes of near-pulp, root dentin, Zn intensity was higher than in ITD remote from the tubules. This increase in Zn2+, as determined by X-ray absorption near edge structure analysis, may indicate the presence of metalloenzymes or transcription factors important to ITD or PTD mineralization. The profiles of the cAp 00.2 X-ray diffraction rings were fitted with a pseudo-Voigt function, and the spatial and azimuthal distribution of these rings' integrated intensities indicated that the cAp platelets were arranged with their c-axes aligned tangential to the edge of the tubule lumen. This texture was continuous throughout the dentin indicating a lack of structural difference between in the Zn rich near-tubular region and the remote ITD. SCANNING 36:231–240, 2014. © 2013 Wiley Periodicals, Inc." @default.
• W1526119469 created "2016-06-24" @default.
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• W1526119469 date "2013-04-29" @default.
• W1526119469 modified "2023-09-22" @default.
• W1526119469 title "Crystallographic texture and elemental composition mapped in bovine root dentin at the 200 nm level" @default.
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• W1526119469 doi "https://doi.org/10.1002/sca.21093" @default.
• W1526119469 hasPubMedCentralId "https://www.ncbi.nlm.nih.gov/pmc/articles/4727833" @default.
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