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- W1527709552 abstract "A chiral ion exchanger, (+)- and (−)-antipodes of 10-camphorsulphonic acid, was applied for the normal-phase solvent-generated molecular complexation chromatography of optical isomers of alkaloids. It was dissolved in the less polar phase of a three-component eluent mixture consisting of solvents having different polarities. Separations were performed on a polar bonded stationary phase (cyanopropylsilica). Remarkably high relative retentions were archieved, permitting rapid chiral separation of different eburnane alkaloids selected as models for the investigations. The influence of mobile phase composition and optical antipode selection of the ion exchanger on the selectivity and efficiency of the separation is discussed. Some applications of the proposed method, including the separation of eight optical isomers of vincamine, are discussed." @default.
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- W1527709552 date "1982-07-01" @default.
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- W1527709552 title "Normal-phase dynamic (solvent-generated) molecular complexation chromatography using anionic ion exchangers" @default.
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- W1527709552 doi "https://doi.org/10.1016/s0021-9673(00)80120-x" @default.
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