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- W1528682332 abstract "Abstract The known selectivity of base-modified silicas for acidic solutes led to development of the in situ tetraalkylammonium hydroxide (TAAH)-modified silica high- performance liquid chromatographic systems described here. These systems are generated by adding small concentrations of TAAH to normal phase eluents pumped through conventional silica columns. The in situ approach has the following advantages: the type and concentration of TAAH can be varied to control separation behavior and selectivity; greater column-to-column consistency and separation reproducibility is achieved; commercially available columns and packings are used; and the TAAH in the mobile phase also serves as an electrolyte for electrochemical detection of solutes, if desired. Retention of 180 solutes spanning several classes of compounds is measured in four different systems; the applicability of this approach to separation of acid concentrates from fuels as well as its compatibility with electrochemical detectors is demonstrated; and in addition, general chromatographic parameters such as the effect of the mobile phase composition on retention and selectivity are discussed." @default.
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- W1528682332 date "1986-01-01" @default.
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- W1528682332 title "Liquid chromatography on silica using mobile phases containing tetraalkylammonium hydroxides" @default.
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- W1528682332 doi "https://doi.org/10.1016/s0021-9673(01)90316-4" @default.
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