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- W1528884744 abstract "The temperature of zeolite samples containing various adsorbed molecules was switchedfrom room temperature to 500–600 K within 30–40 seconds by means of a laser beam. Catalytic n-alkane cracking and H-D exchange with deuterated cyclohexane were monitored by 1H MAS NMR in time steps of down to one second. A two-dimensional representation of the chemical shift and the chemical reaction of the species will be given, allowing a good characterization of reaction steps. At low temperature a weak proton transfer without chemical reaction can be observed, whereas at 430 K and 530 K the proton transfer is accompanied, respectively, by an isomerization or a decomposition to methane and coke. In addition to the effect of high temperature, the laser radiation itself can force the conversion of alkanes to methane and coke." @default.
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- W1528884744 date "1995-01-01" @default.
- W1528884744 modified "2023-10-11" @default.
- W1528884744 title "Laser supported high temperature MAS NMR. A new method for time resolved in situ studies of reaction steps in heterogeneous catalysis" @default.
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- W1528884744 doi "https://doi.org/10.1016/s0167-2991(06)81249-8" @default.
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