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• W1529045195 abstract "Various regulatory authorities like ICH, USFDA, Canadian Drug and Health Agency are emphasizing on the purity requirements and the identification of impurities in Active Pharmaceutical Ingredient’s (API’s). Qualification of the impurities is the process of acquiring and evaluating data that establishes biological safety of an individual impurity; thus, revealing the need and scope of impurity profiling of drugs in pharmaceutical research. Identification of impurities is done by variety of Chromatographic and Spectroscopic techniques, either alone or in combination with other techniques. There are different methods for detecting and characterizing impurities with TLC, HPLC, HPTLC, AAS etc . Conventional Liquid Chromatography, particularly, HPLC has been exploited widely in  field of impurity profiling; the wide range of detectors, and stationary phases along with its sensitivity and cost-effective separation have attributed to its varied applications. Among the various Planar Chromatographic Methods; TLC is the most commonly used separation technique, for isolation of impurities; due to its ease of operation and low cost compared to HPLC. An advancement of thin layer chromatography HPTLC, is a well-known technique for the impurity isolation. Headspace GC is one of the most preferred techniques for identification of residual solvents. The advent of hyphenated techniques has revolutionized impurity profiling, by not only separation but structural identification of impurities as well. Among all hyphenated techniques, the most exploited techniques, for impurity profiling of drugs are LC-MS-MS, LC-NMR, LC-NMR-MS, GC-MS, and LC-MS." @default.
• W1529045195 created "2016-06-24" @default.
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• W1529045195 date "2007-03-15" @default.
• W1529045195 modified "2023-10-13" @default.
• W1529045195 title "Impurity profile: Significance in Active Pharmaceutical Ingredient" @default.
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• W1529045195 doi "https://doi.org/10.12973/ejac/78054" @default.
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