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- W1529851746 abstract "A very sensitive method was developed for detection and confirmation of chloramphenicol (CAP) in equine, porcine and bovine muscle and urine. The method included ethyl acetate extraction of CAP followed by a two-step C18 solid-phase clean up; recovery was >80%. Extracted CAP was determined by liquid chromatography–tandem mass spectrometry (LC–MS/MS) in negative atmospheric pressure chemical ionization mode. LC–MS/MS gave superior sensitivity and selectivity compared to that shown by gas chromatography–mass spectrometry (GC–MS) in electron impact mode. Even in a “dirty” matrix, such as urine, the estimated CAP detection limit for LC–MS/MS detection was 0.02 μg kg−1 while the corresponding value for GC–MS was only 2 μg kg−1." @default.
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- W1529851746 date "2003-04-01" @default.
- W1529851746 modified "2023-10-13" @default.
- W1529851746 title "Determination of chloramphenicol in animal tissues and urine" @default.
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- W1529851746 doi "https://doi.org/10.1016/s0003-2670(02)01566-0" @default.
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