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• W1534650521 abstract "This chapter investigates the synthesis of mordenite in the experimental conditions. The synthesis passes through three main steps. In the first one, the reagents interact at room temperature to form a primary gel. In the second one, a complete reorganization of the gel takes place once the synthesis batch is heated in hydrothermal conditions. In the third step, a slower reorganization in hydrothermal conditions leads to the nucleation and growth of crystalline mordenite. The primary gel presents a texture extremely similar to the source of silica. It seems likely that virtually no dissolution of the source of silica takes place at room temperature, probably due to the preserving effect of a coating of sodium aluminosilicate. The presence of large silica particles with radial compositional heterogeneity can significantly affect the results of some characterization techniques. The aluminium content evaluated by EDX probably represents a surface analysis and overestimates the global composition. The amount of silanols evaluated by 29Si magic angle spinning–nuclear magnet–nuclear magnetic resonance (MAS–NMR) is probably also overestimated, due to the very slow relaxation time of inaccessible 29Si inside the grains of silica. The formation of the hydrothermal gel corresponds to a homogenization of the solid phase and probably occurs through a dissolution–precipitation mechanism in which the memory of the texture of the primary gel is completely lost." @default.
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• W1534650521 date "2005-01-01" @default.
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• W1534650521 title "Amorphous aluminosilicate precursors of mordenite: a case history in the formation of microporosity" @default.
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• W1534650521 doi "https://doi.org/10.1016/s0167-2991(05)80159-4" @default.
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