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- W1535327862 abstract "When 2-amino-3, 4-dihydro-6-phenyl-1, 5-benzodiazocines (1) and 2-amino-5-phenyl-3H-1, 4-benzodiazepines (5) were treated with m-chloroperbenzoic acid, oxidation occurred selectively at the 1-position giving the corresponding 1-oxides (2 and 6), which are a novel class of derivatives of the diazocines and the diazepines. Although reaction of 2 with phosgene afforded the oxadiazolone derivative (4) in high yield, rearrangement of the diazepine oxide (6) occurred upon treatment with phosgene in the presence of imidazoles to form the 3-imidazolyl compound (9). When 6a was treated with acetic anhydride, rearrangement also occurred to give the 3-oxo compound (8)." @default.
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- W1535327862 date "1979-01-01" @default.
- W1535327862 modified "2023-09-23" @default.
- W1535327862 title "Heterocycles. XII. Synthesis of 2-amino-5-phenyl-1,4-benzodiazepine 1-oxides and 2-amino-6-phenyl-1,5-benzodiazocine 1-oxides and their reactions with acylating agents." @default.
- W1535327862 doi "https://doi.org/10.1248/cpb.27.2608" @default.
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