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- W1543288475 abstract "The synthesis of 1-(2-13C)-cyclopropyl-4-phenyl-1,2,3,6-tetrahydropyridine (8) is reported. Attempts were first made to prepare labeled cyclopropylamine via a cyclopropanation/Curtius rearrangement sequence, but the yields were too modest to be suitable for the synthesis of a labeled compound. The preparation of 8 was achieved via cyclopropanation of the N-formyl tetrahydropyridine derivative 21 using the Grignard reagent of ethyl bromide and Ti(O-iPr)4 as a catalyst. The synthesis proceeded in high yield (82%). The method has a wide potential for the synthesis of other cyclopropyl ring labeled and substituted cyclopropyl ring labeled tetrahydropyridine dervatives which can be used in Monoamine Oxidase (MAO) and Cyt P450 enzymes mechanistic studies. Copyright © 2002 John Wiley & Sons, Ltd." @default.
- W1543288475 created "2016-06-24" @default.
- W1543288475 creator A5000350044 @default.
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- W1543288475 date "2002-01-01" @default.
- W1543288475 modified "2023-09-23" @default.
- W1543288475 title "Synthesis of a13C labeledN-cyclopropylamine tetrahydropyridine derivative" @default.
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- W1543288475 doi "https://doi.org/10.1002/jlcr.605" @default.
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