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- W1546103682 abstract "Single crystal X-ray structure determinations are reported for [Os3(CO)11(CNBut)] at 295 K and for [Ru3(CO)11(CNBut)] at ∼ 130 K; both structures are isomorphous with the previously determined room-temperature structure for the latter, which exhibited ∼ 14% disorder in the Ru3 core. Residuals for the present studies were 0.042 and 0.033 for 4491 and 6072 observed reflections respectively. The osmium complex is fully ordered; disorder in the ruthenium complex is reduced to ∼ 6% at low temperature, indicating the disorder to be dynamic rather than a consequence of packing error." @default.
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- W1546103682 date "1986-07-01" @default.
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- W1546103682 title "Cluster chemistry" @default.
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- W1546103682 doi "https://doi.org/10.1016/s0022-328x(00)98958-7" @default.
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