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- W1547524063 abstract "Abstract Compound (I) crystallizes in the space group Pnma with cell constants a = 13.295(2), b = 10.320(1), c = 6.732(1); V = 923.63 A3, d(calc; M = 214.97, z = 4) = 1.546 gm cm−3. Data (2340 total reflections) were collected over the range 4° ≤2θ ≤ 70° and corrected for absorption (μ = 23.804 cm−1). The cation is a cis-chlorohydroxo species in which all the hydrogen atoms were accurately located and refined. Refinement of the heavy atoms with anisotropic thermal parameters and of the hydrogen atom positions (B = 4.0 A2, fixed) led to the final R(F) and Rw(F) factors of 0.033 and 0.039, respectively. Compound (II) crystallizes in the monoclinic space group P21/n with cell constants a = 11.429(2), b = 8.298(2), c = 14.512(2)A, β = 102.25°; V = 1344.895 A3; d(meas., picnometer) = 1.845 gm cm−3, d(calc; M = 771.22, Z = 2) = 1.815 gm cm−3. A total of 3488 unique data were collected over the range 4° ≤2θ ≤ 60°, of which 1976 wee used in the final refinement cycle. The data were corrected for absorption (μ = 1..." @default.
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- W1547524063 date "1993-12-01" @default.
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- W1547524063 title "LIGAND DISPLACEMENT REACTIONS FROM THE COORDINATION SPHERE OF [CIS-CO(NH3)4(NO2)2]NO3: THE CRYSTAL AND MOLECULAR STRUCTURES OF [CIS-CO(NH3)4(OH)CL]CL (I) AND [CO(NH3)4(OXALATO)]2[TRANS-(NH3)(OH)CO(OXALATO)2]·4H2O (II)" @default.
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- W1547524063 doi "https://doi.org/10.1080/00958979308022770" @default.
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