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- W1547655104 abstract "This chapter describes some new applications of 129Xe NMR spectroscopy that use the dynamic properties of adsorbed xenon to learn about structure of pores, xenon exchange and diffusion. Exchange rates, obtained with 2D EXSY NMR techniques, are measured for diffusion paths with widely varying length scales as demonstrated for intraparticle exchange in Na Mordenite, and interparticle exchange in mixed NaX and NaY zeolites. The observation of distinct clusters of up to 8 xenon atoms in AgA zeolite and intercluster exchange has given information on the location of silver ions and residual water. The observation of anisotropic chemical shifts in sieves, such as ALPO- 11, ALPO-5, ALPO-8, VPI-5, SSZ-24 and ZSM- 12, along with 2D-EXSY NMR data, has allowed modeling of the distribution of xenon atoms in these low-dimensional pore systems. The model systems chosen to illustrate the effects of xenon exchange on microscopic and macroscopic scales were Na-Mordenite and mixtures of NaX and NaY zeolites. AgA zeolite provides an example of a system with very slow xenon exchange. 1D spectra show distinct populations of xenon clusters in different cages." @default.
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- W1547655104 date "1995-01-01" @default.
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- W1547655104 title "2D EXSY 129Xe NMR: New possibilities for the study of structure and diffusion in microporous solids" @default.
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- W1547655104 doi "https://doi.org/10.1016/s0167-2991(06)81895-1" @default.
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